5 ways to help you identify common fibers



With the continuous advancement of textile production technology, more and more new fibers have become the raw materials of textiles, which has brought about the problem of identif…

With the continuous advancement of textile production technology, more and more new fibers have become the raw materials of textiles, which has brought about the problem of identifying fibers for textiles. Commonly used fiber identification methods include microscopic observation, combustion, reagent color development, dyeing, dissolution, etc.

1 Microscopic observation method

Make longitudinal slices and cross-sectional slices of the fibers, observe the longitudinal and transverse morphology of the fibers under a microscope, and identify the fibers based on differences in morphological characteristics, see Table 1.

Table 1 Morphological characteristics of various fibers

Fiber types

Vertical form

Cross-sectional shape

Tencel fiber

smooth

More regular round or oval shape, with skin and core layer

Modal fiber

There are 1 to 2 grooves in the longitudinal direction

Irregular, similar to a round waist, smoother, with a skin core

Soy fiber

The surface has irregular grooves and island-like concavities

Flat dumbbell shape and round waist

Bamboo fiber

There are grooves on the surface

Zigzag type, with skin and core layer

Chitin fiber

There are obvious grooves on the surface

The edge is jagged and the core layer has obvious small gaps

Viscose fiber

There are grooves on the surface

Zigzag type, with skin and core layer

Cotton fiber

There are natural twists

The waist is round with a middle cavity

Silk

Smooth surface

Irregular triangle

Wool fiber

There are scales on the surface

Circle

Polyester fiber

Rod-shaped

Smooth round surface

2 Combustion method

Different fibers have different flames, smoke, odors, residues, etc. during the burning process. Therefore, fiber types can be distinguished according to the characteristics of the fibers during and after burning, as shown in Table 2.

Table 2 Characteristics of various fibers during and after combustion

Fiber types

Close to the flame

In flames

Leave the flame

Burning smell

Residue form

Tencel fiber

Does not melt or shrink

Burn quickly

Keep burning

The smell of burning paper

Gray black gray

Modal fiber

Does not melt or shrink

Burn quickly

Keep burning

The smell of burning paper

Gray black gray

Soy protein fiber

Shrink

It does not melt when burning, but has black smoke

Not easy to burn

Burning hair smell

Crunchy black ash

Bamboo fiber

Does not melt or shrink

Burn quickly

Keep burning

The smell of burning paper

Gray black gray

Chitin fiber

Does not melt or shrink

Burn quickly

Keep burning

The smell of burning paper

Gray black gray

Viscose fiber

Does not melt or shrink

Burn quickly

Keep burning

The smell of burning paper

A small amount of off-white ash

Cotton fiber

Does not melt or shrink

Burn quickly

Keep burning

The smell of burning paper

A small amount of off-white ash

Silk

Shrink

Gradually burning

Not easy to burn

Burning hair smell

Crunchy black ash

Wool fiber

Shrink

Gradually burning

Not easy to burn

Burning hair smell

Crunchy black ash

Polyester fiber

Shrinkage melt

Melt first and then burn, with solution dripping

Can spread burning

Special aroma

Glassy dark brown hard ball

3 Reagent color development method

Since the structures of various fibers are different, they have different coloring reactions to iodine and potassium iodide solutions. The fibers can be identified by observing the color and swelling of the fibers after the action of the reagents. This identification only applies to white fibers, and colored fibers must fade before testing can be conducted. Reagent preparation: Dissolve 20 grams of iodine in 100 ml of saturated potassium iodide solution, mix thoroughly, and then soak the fiber for 1 minute. After sufficient washing, judge according to its color, see Table 3.

Table 3 Coloring reactions of various fiber burning to iodine solution

Fiber types

Tencel fiber

Modal fiber

Soy protein fiber

Bamboo fiber

Chitin fiber

Color development in iodine solution

Black, blue and green

Blue gray

Brown

Blue gray

Black

Types of fiber

Viscose fiber

Cotton fiber

Silk

Wool fiber

Polyester fiber

Color development in iodine solution

Black, blue and green

No staining

Light yellow

Light yellow

No staining

4 staining methods

The dyeing method is used to identify fibers, mainly based on the different color reactions of various fibers to dyes. There are two types of dyeing methods: cold dyeing and boiling dyeing. The recipe of the dyeing method is shown in Table 4.

Table 4 Dyeing method formula

Cold dyeing

Boiling dyeing method

Dyes

Weight (g)

Dyes

Weight (g)

Direct Indigo 2B

2.5

Acid fuchsin 6B

1

Acid fuchsin 6B

3

Salt base light yellow (thick)

1

Picric acid

5

Disperse blue GF

0.5

Tannin

5

Pancreas plus bleach T

0.5

Pour the formula in Table 4 into 50 ml of ethanol and stir until dissolved, then dilute to 500 ml with distilled water for later use. The cold dyeing method directly puts the fiber into the solution for dyeing, then rinses the fiber with cold water, squeezes out the water, and observes the color for identification; the boiling dyeing method puts the fiber into the solution for dyeing, boils it for 3 minutes, rinses it 3 times, and then puts it into 0.1 % of the pancreas plus bleaching T solution, squeeze out the water, and observe the color for identification. The dyeing reactions of various fibers are shown in Table 5.

Table 5 Dyeing reactions of various fibers

Fiber types

Cold dyeing method

Boiling dyeing method

Cotton fiber

Purple

Earthy yellow

Viscose fiber

Red purple

Light yellow

Vinyl

Light yellow-green

Dark olive green

Acrylic

No color

Light yellow

Polyester

No color

Light sky blue

Nylon

Light yellow

Dark grass green

5 Dissolution method

The dissolution method is an effective method to identify various fibers. The principle is to use the dissolution characteristics of various fibers in different chemical solvents and at different temperatures to determine their varieties. The fibers to be identified can be put into a test tube, inject a certain solvent, stir with a glass rod, and observe the dissolution of the fibers. If the amount of fiber is very small, you can also put the sample into the concave surface with a concave slide, add solvent, cover the slide, and observe directly under the microscope. Using dissolution method to identify fibersAt this time, the concentration of the solvent and the heating temperature should be strictly controlled, and the dissolution speed of the fiber should be paid attention to. Using the dissolution method requires an accurate understanding of the chemical properties of various fibers, and the inspection procedures are also complicated. The microscopic observation method and combustion method are more intuitive, but inspectors must have rich practical experience; the reagent colorimetric method and staining method are more complicated to operate and can be used under special circumstances.

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